Optical–chemical sensors based on optical fibers can be made in reflection or transmission schemes. In the reflection scheme, the sensing area is typically present at the end of the fiber, and the light source and the detector are placed on the same side of the fiber. This approach can be exploited to achieve chemical probes useful in several application fields where remote sensing is required. In this work, to obtain an extrinsic optical fiber chemical sensor in a reflection scheme, two optical fibers are used to monitor a chemically sensitive region achieved by a C-shaped waveguide with a molecularly imprinted polymer (MIP) as a core between the optical fibers. The proposed micrometer-sized probe is developed and tested as a proof of concept via a MIP for 2-Furaldehyde (2-FAL) detection of interest in food and industrial applications. The experimental results of the proposed sensing approach showed several advantages, such as a nanomolar detection limit and an ultra-wide concentration detection range due to different kinds of MIP recognition sites in the optical path between the fibers.
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